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:: دوره 31، شماره 3 - ( پائيز 1400 ) ::
جلد 31 شماره 3 صفحات 265-259 برگشت به فهرست نسخه ها
تهیه و ارزیابی نانوذرات اکسید بیسموت توسط تخریب حرارتی چارچوب فلز-آلی
نگار معتکف کاظمی
استادیار، گروه نانوفناوری پزشکی، دانشکده علوم و فناوری‌های نوین، علوم پزشکی تهران، دانشگاه آزاد اسلامی، تهران، ایران ، negar.motakrf@gmail.com
چکیده:   (386 مشاهده)
چکیده
سابقه و هدف: چارچوب­های فلز-آلی به دلیل حجم حفره بالا، شبکه حفره منظم، مساحت سطح بالا، حضور همزمان گروه­های آلی و معدنی پتانسیل کاربردی گسترده دارند. امروزه تهیه نانوذرات اکسید فلزی با روش تخریب حرارتی چارچوب­های فلز-آلی گسترش یافته است. هدف از این تحقیق تهیه نانوذرات اکسید بیسموت با روش تخریب حرارتی برای حذف بخش آلی از چارچوب فلز-آلی بر پایه فلز بیسموت بود.
روش بررسی: نانوذرات اکسید بیسموت توسط پراش پرتو ایکس (XRD) برای تعیین ساختار بلوری، طیف­سنجی مادون قرمز تبدیل فوریه (FTIR) برای ارزیابی گروه­های عاملی، میکروسکوپ الکترونی روبشی (SEM) و میکروسکوپ الکترونی عبوری (TEM) برای مطالعه اندازه و شکل، طیف سنجی توزیع انرژی پرتوی ایکس (EDS) برای بررسی ترکیب شیمیایی، و طیف­سنجی بازتاب انتشاری (DRS) جهت تعیین جذب اشعه ماوراء بنفش و گاف انرژی بررسی شدند. فعالیت ضدباکتری این نانوذرات علیه باکتری گرم منفی سالمونلا تیفی موریوم و گرم مثبت استافیلوکوکوس اورئوس ارزیابی شد. 
یافته ها: نانوذرات بلوری اکسید بیسموت به صورت کروی شکل و یکدست توسط روش تخریب حرارتی چارچوب فلز-آلی بر پایه فلز بیسموت تهیه شد. کاربردهای بالقوه این نانوذرات می­تواند باعث گسترش کاربردهای حوزه علوم پزشکی شود.
نتیجه­ گیری: نتایج نشان می­دهد که نانوذرات اکسید بیسموت دارای سد کنندگی اشعه ماوراء بنفش و فعالیت ضدباکتری هستند و می­توانند پتانسیل خوبی برای کاربردهای مختلف به ویژه در زمینه ­های پزشکی، دارویی، غذایی، و آرایشی و بهداشتی داشته باشند.
واژه‌های کلیدی: چارچوب فلز-آلی، نانوذرات اکسید بیسموت، تخریب حرارتی، ضدباکتری، سدکنندگی اشعه ماوراء بنفش
متن کامل [PDF 568 kb]   (181 دریافت)    
نيمه آزمايشي : تجربي | موضوع مقاله: شیمی
دریافت: 1398/9/10 | پذیرش: 1399/1/30 | انتشار: 1400/6/10
فهرست منابع
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80. Gotić M, Popović S, and Musić S. Influence of synthesis procedure on the morphology of bismuth oxide particles. Mater Lett 2007; 61:709-714. [DOI:10.1016/j.matlet.2006.05.048]
81. Sood S, Umar A, Mehta SK, and Kansal SK. α-Bi2O3 nanorods: An efficient sunlight active photocatalyst for degradation of Rhodamine B and 2,4,6-trichlorophenol. Ceram Int 2015; 41:3355-3364. [DOI:10.1016/j.ceramint.2014.10.038]
82. Leontiea L, Caraman M, Alexe M, and Harnagea C. Structural and optical characteristics of bismuth oxidethin films. Surf Sci 2002; 507-510:480-485. [DOI:10.1016/S0039-6028(02)01289-X]
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Motakef Kazemi N. Preparation and evaluation of bismuth oxide nanoparticles by thermal degradation of metal organic framework. MEDICAL SCIENCES. 2021; 31 (3) :259-265
URL: http://tmuj.iautmu.ac.ir/article-1-1668-fa.html

معتکف کاظمی نگار. تهیه و ارزیابی نانوذرات اکسید بیسموت توسط تخریب حرارتی چارچوب فلز-آلی. فصلنامه علوم پزشکی. 1400; 31 (3) :265-259

URL: http://tmuj.iautmu.ac.ir/article-1-1668-fa.html



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دوره 31، شماره 3 - ( پائيز 1400 ) برگشت به فهرست نسخه ها
فصلنامه علوم پزشکی دانشگاه آزاد اسلامی واحد پزشکی تهران Medical Science Journal of Islamic Azad Univesity - Tehran Medical Branch
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